Antibacterial activities of triterpenoidal compounds isolated from Calothamnus quadrifidus leaves

Table 1 The ¹H-NMR (600 MHz) and ¹³C-NMR (150 MHz) data of compound 1 and 3–5 (in DMSO); δ in ppm; J in Hz

Position	1		3		4		5
Position	δC	δH	δC	δH	δC	δH	δC	δH
1	38.84		38.20		39.38		40.75
2	27.61		27.55		67.43		67.66
3	77.14	3.39 (1 H, brs)	82.52	3.83 (1 H, s)	77.30	3.62 (1 H, brs)	82.65	3.62 (1 H, brs)
4	38.93		38.87		38.87		40.40
5	55.25		55.17		55.87		55.87
6	18.42		18.43		18.46		77.35	2.13 (1 H, m)
7	34.37		34.45		36.82		40.40
8	40.66		40.49		40.40		39.38
9	50.36		50.32		48.97		48.97
10	37.18		37.22		38.02		38.02
11	20.91		20.91		21.54		22.61
12	25.52		25.47		25.56		23.81
13	38.04		38.04		38.95		38.95
14	42.45		42.45		42.48		42.48
15	30.55		30.55		31.81		30.85
16	32.16		32.16		32.17		32.17
17	55.94		55.84		55.87		55.87
18	47.07		47.02		47.07		47.07
19	49.07		48.97		48.93		48.97
20	150.82		150.67		150.37		150.60
21	29.66		29.53		29.09		29.28
22	36.80		36.70		36.81		36.81
23	28.55	1.32 (3 H, s, Me)	63.21	3.70 (2 H, s)	62.87	3.69 (2 H, s)	63.26	3.70 (2 H, s)
24	16.17	1.11 (3 H, s, Me)	16.42	1.32 (3 H, s, Me)	17.35	1.32 (3 H, s, Me)	17.35	1.38 (3 H, s, Me)
25	16.27	0.87 (3 H, s, Me)	17.37	0.91 (3 H, s, Me)	17.58	0.81 (3 H, s, Me)	17.58	0.76 (3 H, s, Me)
26	16.41	0.77 (3 H,s, Me)	17.60	1.07 (3 H,s, Me)	16.48	0.96 (3 H,s, Me)	18.46	1.08 (3 H,s, Me)
27	14.84	0.93 (3 H, s, Me)	16.14	1.08 (3 H, s, Me)	14.80	0.71 (3 H, s, Me)	14.80	0.82 (3 H, s, Me)
28	177.72	12.03 (1 H, brs)	177.60	12.03 (1 H, brs)	177.98	12.07 (1 H, brs)	177.75	12.04 (1 H, brs)
29	110.11	4.69 (1 H, brs, H-29^a) 4.56 (1 H, brs, H-29^b)	109.96	4.69 (1 H, brs, H-29^a) 4.57 (1 H, brs, H-29^b)	109.21	4.69 (1 H, brs, H-29^a) 4.57 (1 H, brs, H-29^b)	110.10	4.69 (1 H, brs, H-29^a) 4.57 (1 H, brs, H-29^b)
30	19.39	1.65 (3 H,s, Me)	19.39	1.65 (3 H,s, Me)	19.40	1.65 (3 H,s, Me)	19.40	1.65 (3 H,s, Me)
31			172.53
32			21.55	1.91 (3 H,s, Me)

ISSN: 2662-7671