Table 4 1H- and 13C-NMR spectroscopic data for 6 and 7
|  | Dihydrodehydrodiconiferyl alcohol 4-O-β-D-glucoside (6) | Dihydrodehydrodiconiferyl alcohol 9-O-β-D-glucoside (7) | ||
|---|---|---|---|---|
δ C | δH (Mult, Int), J in Hz | δ C | δH (Mult, Int), J in Hz | |
1 | 137.09 | Â | 134.67 | Â |
2 | 111.19 | 7.03 (d, 1H), 1.84 | 110.71 | 7.02 (d, 1H), 2.01 |
3 | 150.9 | Â | 149.05 | Â |
4 | 147.6 | Â | 147.48 | Â |
5 | 117.95 | 7.14 (d, 1H), 8.43 | 116.08 | 6.78 (d, 1H), 8.09 |
6 | 119.37 | 6.93 (dd, 1H), 8.31, 2.03 | 119.72 | 6.89 (dd, 1H), 8.28, 2 |
7 | 88.48 | 5.56 (d, 1H), 5.85 | 88.98 | 5.62 (d, 1H), 6.21 |
8 | 55.68 | 3.44 (m, 1H) | 53.28 | 3.69 (m, 1H) |
9 | 65.07 | 3.80, 3.75 (m, m, 2H) | 72.46 | 4.23, 3.79 (dd, m, 2H) |
3-OCH3 | 56.79 | 3.87 (s, 3H) | 56.44 | 3.85 (s, 3H) |
1′ | 138.37 |  | 136.64 |  |
2′ | 114.19 | 6.73 (s, 1H) | 114.19 | 6.75 (s, 1H) |
3′ | 145.24 |  | 145.21 |  |
4′ | 147.6 |  | 147.48 |  |
5′ | 129.58 |  | 129.56 |  |
6′ | 118.04 | 6.72 (s, 1H) | 118.21 | 6.80 (s, 1H) |
7′ | 32.89 | 2.63 (t, 2H) | 32.89 | 2.65 (t, 2H) |
8′ | 35.84 | 1.82 (m, 2H) | 35.82 | 1.84 (m, 2H) |
9′ | 62.22 | 3.57 (t, 2H) | 62.23 | 3.59 (t, 2H) |
3′-OCH3 | 56.71 | 3.83 (s, 3H) | 56.77 | 3.88 (s, 3H) |
1″ | 102.78 | 4.88 (covered by solvent, 1H) | 104.57 | 4.38 (d, 1H), 7.79 |
2″ | 74.90 | 3.48 (m, 1H) | 75.18 | 3.25 (m, 1H) |
3″ | 77.84 | 3.39 (m, 1H) | 78.07 | 3.31 (m, 1H) |
4″ | 71.34 | 3.39 (m, 1H) | 71.66 | 3.31 (m, 1H) |
5″ | 78.19 | 3.39 (m, 1H) | 78.26 | 3.31 (m, 1H) |
6″ | 62.51 | 3.85, 3.69 (m, 2H) | 62.81 | 3.88, 3.70 (m 2H) |