Table 1 NMR Spectroscopic data for acthaside

1

-

-

2

-

166.7, C

3

5.94, (d, 0.7)

111.6, CH

4

-

181.7, C

4a

-

115.3, C

5

-

144.0, C

6

6.65 (d, 2.4)

119.8, CH

7

-

161.8, C

8

6.62 (d, 2.4)

102.6, CH

8a

-

163.1, C

9

2.97 (dd, 12.1, 7.4)

3.68 (dd, 12.1, 5.3)

43.3, CH₂

10

4.06 (m)

76.9, CH

11

1.09 (d, 6.2)

21.5, CH₃

12

2.25 (d, 0.7)

19.9, CH₃

1′

4.45 (d, 8.0)

103.0, CH

2′

3.07 (dd, 8.7, 8.0)

75.5, CH

3′

3.27 (m)

78.3, CH

4′

3.20 (m)

71.9, CH

5′

3.21 (m)

77.9, CH

6′

3.58 (m)

3.75 (dd, 11.8, 1.6)

62.9, CH₂